HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxypropyl 4-methylbenzenesulfonate → HCID 69140635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxypropyl 4-methylbenzenesulfonate | HCID 13522988 | — |
| Reactant | HCID 69141315 | HCID 69141315 | — |
| Product | HCID 69140635 | HCID 69140635 | 94% |
Reaction Steps
This compound was prepared from (R)-2-ethyl-piperazine-1,4-dicarboxylic acid 4-tert-butyl ester 1-(2-fluoro-5-hydroxy-benzyl) ester and toluene-4-sulfonic acid 3-methoxy-propyl ester according to the procedure described in Example 187 to give the product as a colorless oil (342 mg; 94%); MS (ISP): 472.4 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07022707B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-c16d5d61c34d44b89e0a42087ff3a134 |
| Source note | uspto-grants-2006_04 |