HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethylcyclopropane → 2-Chloro-4-cyclopropylmethoxy-6-fluoro-benzylalcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Reactant | 3-Chloro-5-fluoro-4-(hydroxymethyl)phenol | HCID 22220009 | — |
| Product | 2-Chloro-4-cyclopropylmethoxy-6-fluoro-benzylalcohol | HCID 22220058 | 77% |
Reaction Steps
This compound was prepared from 3-Chloro-5-fluoro-4-hydroxymethyl-phenol and cyclopropylmethylbromide according to the procedure described in Example 179 to give the product as a yellowish oil (305 mg, 77%); MS (EI): 230.1 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07022707B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-2b10bbcdbd6b4d1e862ff81dc0a6f436 |
| Source note | uspto-grants-2006_04 |