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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1794163Generated: November 4, 2026

4-Allyloxy-2-chloro-6-fluoro-benzylalcohol → HCID 69141168, compound

https://huagongshe.com/reaction/1794163

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Allyloxy-2-chloro-6-fluoro-benzylalcoholHCID 22220080—
Reactant(R)-4-Chlorocarbonyl-3-ethyl-piperazine-1-carboxylic acid tert-butyl esterHCID 86586001—
ProductHCID 69141168HCID 6914116887%

Reaction Steps

This compound was prepared from 4-allyloxy-2-chloro-6-fluoro-benzylalcohol and (R)-4-chlorocarbonyl-3-ethyl-piperazine-1-carboxylic acid tert-butyl ester according to the procedure described in Example 179 to give the product as a colorless oil (405 mg; 87%); MS (ISP): 474.4 (M+NH4)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07022707B2
Source datasetuspto-grants-2006_04
ORD IDord-62b06560a73f46cd914cfe75367bf2e8
Source noteuspto-grants-2006_04