HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethyl methyl ether → 2-Chloro-6-fluoro-4-(2-methoxy-ethoxy)-benzylalcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | 3-Chloro-5-fluoro-4-(hydroxymethyl)phenol | HCID 22220009 | — |
| Product | 2-Chloro-6-fluoro-4-(2-methoxy-ethoxy)-benzylalcohol | HCID 22220010 | 52% |
Reaction Steps
This compound was prepared from 3-chloro-5-fluoro-4-hydroxymethyl-phenol and (2-bromoethyl) methyl ether according to the procedure described in Example 179 to give the product as a yellowish oil (209 mg, 52%); MS (EI): 234.1 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07022707B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-006228abd25348f399201f56147c917e |
| Source note | uspto-grants-2006_04 |