1-(2-Pyridyl)piperazine → HCID 69642583, compound

HRID 1794173Notes

Reaction equation

HRID 1794173 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[N:7]1[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]1.Cl.[CH2:14]([O:16][C:17]1[CH:18]=[C:19]([C:26]2[C@@H:35]3[C@@H:30]([CH2:31][CH:32]=[CH:33][CH2:34]3)[C:29](=[O:36])[N:28]([C:37]3[CH:42]=[CH:41][C:40]([C:43](N4CCN(C5C=CC=CC=5)CC4)=[O:44])=[CH:39][CH:38]=3)[N:27]=2)[CH:20]=[CH:21][C:22]=1[O:23][CH2:24][CH3:25])[CH3:15]>C(OCC)C>[CH2:14]([O:16][C:17]1[CH:18]=[C:19]([C:26]2[C@@H:35]3[C@@H:30]([CH2:31][CH:32]=[CH:33][CH2:34]3)[C:29](=[O:36])[N:28]([C:37]3[CH:38]=[CH:39][C:40]([C:43]([N:10]4[CH2:9][CH2:8][N:7]([C:2]5[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=5)[CH2:12][CH2:11]4)=[O:44])=[CH:41][CH:42]=3)[N:27]=2)[CH:20]=[CH:21][C:22]=1[O:23][CH2:24][CH3:25])[CH3:15]

Participants

4

Reactant 2

HCID 944591-(2-Pyridyl)piperazineHCID 69641867HCID 69641867, compound

Product 1

HCID 69642583HCID 69642583, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Prepared from intermediate product A1 and 1-(2-pyridyl)piperazine as described for compound 1. Cystallised from diethyl ether as the free base. M.p. 183–184° C.

Sources & evidence

ORD record
ord-9e563d6208264ad3b3a8ab905aa26f60
Source dataset
uspto-grants-2006_04
Patent number
US07022696B2

Reaction notes

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