(1,1'-Biphenyl)-4-carboxaldehyde → HCID 10183470, compound

HRID 1794194Notes

Reaction equation

[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][NH:6]2.[C:11]1([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:16]=[CH:15][C:14]([CH:17]=O)=[CH:13][CH:12]=1>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[C:4]([CH:17]([C:4]1[C:3]3[C:7](=[CH:8][CH:9]=[CH:10][C:2]=3[Cl:1])[NH:6][CH:5]=1)[C:14]1[CH:15]=[CH:16][C:11]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)=[CH:12][CH:13]=1)=[CH:5][NH:6]2

Participants

Reactant 2

HCID 76689(1,1'-Biphenyl)-4-carboxaldehyde

HCID 913454-Chloroindole

Product 1

HCID 10183470HCID 10183470, compound

Procedure

The compound Bis(4-chloroindol-3-yl)-(1,1′-biphenyl-4-yl)methane was prepared following general procedure A, starting from 4-chloro indole and 4-biphenyl carboxaldehyde. LC: Tr 2.79 min, MS: 467 (M+H)+

Workup

customTr 2.79 min, MS

Sources & evidence

ORD record: ord-2a278dfab41c45b483bcf914bc55a33c
Source dataset: uspto-grants-2006_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07022730B2

Reaction notes

Loading…