1-Methylindole → Bis(1-methylindol-3-yl)-(1,1'-biphenyl-4-yl)methane

HRID 1794204Notes

Reaction equation

HRID 1794204 reaction equation
[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3]1.[C:11]1([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:16]=[CH:15][C:14]([CH:17]=O)=[CH:13][CH:12]=1>>[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]([CH:17]([C:4]2[C:5]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[N:2]([CH3:1])[CH:3]=2)[C:14]2[CH:15]=[CH:16][C:11]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)=[CH:12][CH:13]=2)=[CH:3]1

Participants

3

Reactant 2

HCID 117811-MethylindoleHCID 76689(1,1'-Biphenyl)-4-carboxaldehyde

Product 1

HCID 10180866Bis(1-methylindol-3-yl)-(1,1'-biphenyl-4-yl)methane

Procedure

The compound Bis(1-methylindol-3-yl)-(1,1′-biphenyl-4-yl)methane was prepared following procedure A, starting from N-methyl indole and 4-biphenyl carboxaldehyde. LC: Tr 2.92 min, MS: 427 (M+H)+

Workup

  1. customTr 2.92 min, MS

Sources & evidence

ORD record
ord-e16e3fdf47664e9e950c15191f1b5cb4
Source dataset
uspto-grants-2006_04
Patent number
US07022730B2

Reaction notes

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