Benzyl Bromide → HCID 10145164, compound

HRID 1794205Notes

Reaction equation

HRID 1794205 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][NH:6]2.[CH2:11](Br)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.O[CH2:20][C:21]1[O:27][C:24]([CH:25]=[O:26])=[CH:23][CH:22]=1>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[C:4]([CH:20]([C:4]1[C:3]3[C:7](=[CH:8][CH:9]=[CH:10][C:2]=3[Cl:1])[N:6]([CH2:4][C:3]3[CH:7]=[CH:8][CH:9]=[CH:10][CH:2]=3)[CH:5]=1)[C:21]1[O:27][C:24]([CH2:25][OH:26])=[CH:23][CH:22]=1)=[CH:5][N:6]2[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 3

HCID 7498Benzyl BromideHCID 913454-ChloroindoleHCID 2373325-(Hydroxymethyl)furfural

Product 1

HCID 10145164HCID 10145164, compound

Procedure

The compound Bis(4-chloro-1-benzylindol-3-yl)-(5-hydroxymethyl-2-furyl)methane was prepared following procedure B, starting from 4-chloro indole and benzylbromide, and the resulting compound was reacted with 5-hydroxy methyl furfural following general procedure A. LC: Tr 2.89 min, MS: 591 (M+H)+

Workup

  1. customTr 2.89 min, MS

Sources & evidence

ORD record
ord-307db784897146e6be8237b6630244ce
Source dataset
uspto-grants-2006_04
Patent number
US07022730B2

Reaction notes

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