HCID 22221589, compound → HCID 22221592, compound

Participants

Reaction Steps

2-[5-Methoxy-2-(4-methoxy-phenyl)-benzofuran-7-yl]-propan-2-ol 115 (0.4 g, 1.3 mmol) and Burges Reagent (0.4 g, 1.7 mmol) in THF (10 ml) were heated to reflux. After 30 min, the reaction was cooled, concentrated and the product was purified by column chromatography on silica gel (10% Et OAc/Hexane) to give 116 as a solid (0.29 g, 77%).

Provenance & Evidence