HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → Benzenesulfonyl hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Product | Benzenesulfonyl hydrazide | HCID 65723 | — |
Reaction Steps
Benzenesulfonohydrazide is prepared from benzenesulfonyl chloride (500 mg, 2.83 mmol) and hydrazine monohydrate (0.42 mL, 8.49 mmol) according to the experimental provided in Tetrahedron 2002, 58, 5513. The product is recrystallized from EtOAc/Hexane. The yield is 136 mg of benzenesulfonohydrazide, 28%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07026339B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-aa0c24f882f845a5b42ee00e2015d391 |
| Source note | uspto-grants-2006_04 |