HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 22217724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 5-Acetamidonaphthalene-1-sulfonyl chloride | HCID 5010306 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22217724 | HCID 22217724 | — |
Reaction Steps
1.10 g of 5-acetylaminonaphthalene-1-sulfonyl chloride is dissolved in 8 mL of ethanol and 8 mL of methylamine solution in ethanol are added dropwise. Then the resulting mixture is stirred at reflux temperature for 3.5 hours and the solvent is distilled off in vacuo. The residue is purified by chromatography. Yield: 0.50 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07026475B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-c1313fc8d512488a9ada1cbece861b4f |
| Source note | uspto-grants-2006_04 |