HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10075512, compound → HCID 10320163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10075512 | HCID 10075512 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 10320163 | HCID 10320163 | — |
Reaction Steps
A suspension of {2-[2-(1-methyl-5-naphthalen-2-yl-6-oxo-1,6-dihydro-[4,4′]bipyridinyl-2-yl)-pyrrolidin-1-yl]-ethyl}-carbamic acid tert-butyl ester (100 mg, 0.19 mmol) in sat. HCl in EtOAc was stirred at RT for 4 h. Then the title compound was isolated by filtration and washed with dry EtOAc. MS (ES+): 425 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07026326B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-39d9f8da757844b2991e6d639add8164 |
| Source note | uspto-grants-2006_04 |