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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 17956Generated: October 25, 2026

p,p'-Dimethoxybenzhydryl alcohol → 4-(4,4'-Dimethoxybenzhydryl)-thiophenyl boronic acid

https://huagongshe.com/reaction/17956

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp,p'-Dimethoxybenzhydryl alcoholHCID 69768—
Reactant4-Mercaptophenylboronic acidHCID 4431894—
SolventAcetic AcidHCID 176—
Product4-(4,4'-Dimethoxybenzhydryl)-thiophenyl boronic acidHCID 67120687—

Reaction Conditions

Temperature60 °C

Reaction Steps

4,4′-Dimethoxybenzhydrol (2.7 g, 11 mmol) and 4-mercaptophenylboronic acid (1.54 g, 10 mmol) were dissolved in 20 mL AcOH and heated at 60° C. for 1 h. Solvent was evaporated and the residue was dried under high vacuum. This material was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07741321B2
Source datasetuspto-grants-2010_06
ORD IDord-de4daeb7cd904fa48710066dc68f64ce
Source noteuspto-grants-2010_06