HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 10272566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22180855 | HCID 22180855 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10272566 | HCID 10272566 | — |
Reaction Steps
hydrochloride (107 mg, 25%) was obtained as a yellow solid after crystallisation from ethanol by reacting a solution of 5-[6,7-dimethoxy-2-(2-phenyl-[1,3]dioxolan-2-yl)-benzofuran-4-ylmethyl]-pyrimidine-2,4-diamine (440 mg, 0.981 mmol) in ethanol with 6 N HCl for 16 h at r.t.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07030130B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-8fd5cd8a3dbf4735b6874eb868e15e39 |
| Source note | uspto-grants-2006_04 |