HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-methylbenzenesulfonyl chloride → HCID 10297515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| Reactant | N-(2-Amino-4,5,6,7-tetrahydro-1,3-benzothiazol-6-yl)propanamide | HCID 22180927 | — |
| Product | HCID 10297515 | HCID 10297515 | — |
Reaction Steps
The title compound was prepared from N-(2-amino-4,5,6,7-tetrahydro-1,3-benzothiazol-6-yl)propanamide (47 mg, 0.21 mmol) and 2,4-dichloro-6-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (20.3 mg) with purity >90%. MS (pos) m/z 448.1, 450.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07030135B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-cb83fa3d00d742b7911c5036706b73a1 |
| Source note | uspto-grants-2006_04 |