HRID1796289

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：CO[C@@H]1C[C@H](C(=O)Nc2ccc(N3CCCCC3=O)cc2F)N(C(=O)OC(C)(C)C)C1

HCID11154790

未命名化合物

PRODUCTS

生成物

结构：CO[C@H]1CN[C@@H](C(=O)Nc2ccc(N3CCCCC3=O)cc2F)C1

HCID11416392

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Into a solution of 8 (0.329 g, 0.761 mmol) in anhydrous CH2Cl2 (5 mL) was added TFA (5 mL). The solution was stirred at RT for 0.5 h before concentrating under reduced pressure to reveal 9 (0.255 g, 100%) as a tan oil.

WORKUP

后处理

concentrationbefore concentrating under reduced pressure