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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1796458Generated: October 30, 2026

HCID 22181383, compound → HCID 22181438, compound

https://huagongshe.com/reaction/1796458

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22181383HCID 22181383—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 22181438HCID 22181438108.4%

Reaction Steps

Following general procedure 2C: A mixture of N,N-diethyl-4-(methylamino)-3-nitrobenzamide (0.130 g, 0.517 mmol) and 10% Pd/C in EtOAc (10 mL) was hydrogenated at 40 psi. Usual work-up provided the title compound (0.124 g) which was used without further purification. MS (ESI) (M+H)+=222.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07030139B2
Source datasetuspto-grants-2006_04
ORD IDord-fdfc1ef3ef324fc9bf9883a2554b2b24
Source noteuspto-grants-2006_04