HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22181313, compound → HCID 22181329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22181313 | HCID 22181313 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22181329 | HCID 22181329 | 89.6% |
Reaction Steps
Following general procedure 2C: N-{4-[(cyclopropylmethyl)amino]-3-nitrophenyl}acetamide (7.0 g, 28 mmol) was hydrogenated in ethyl acetate (300 mL) with 10% Pd/C (0.8 g) at 25 psi H2 in Parr shaker. After work up, isolated the desired product (5.5 g, 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07030139B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-a2d1bb4d8bc64a72a77591d450f5af2b |
| Source note | uspto-grants-2006_04 |