Hydroxylamine → HCID 178513433, compound

HRID 1796659Notes

Reaction equation

HRID 1796659 reaction equation
[N:1]1([C:7]#[N:8])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[NH2:9][OH:10]>>[OH:10][NH:9][C:7]([N:1]1[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1)=[NH:8]

Participants

3

Reactant 2

HCID 787HydroxylamineHCID 737384-Morpholinecarbonitrile

Product 1

HCID 178513433HCID 178513433, compound

Procedure

The title compound was prepared from the reaction of morpholine nitrile and hydroxylamine (equimolar amounts) by a route analogous to that used for the preparation of Example 412A to yield 419A in quantitative yield. 1H NMR (400 MHz, DMSO-d6) δ 8.33 (s, 1H), 5.18 (S, 2H), 3.57 (m, 4H), 2.93 (m, 4H)

Workup

  1. customthat used for the preparation of Example 412A

Sources & evidence

ORD record
ord-75f4cb47893848418cf9fc1937a54697
Source dataset
uspto-grants-2006_04
Patent number
US07030112B2

Reaction notes

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