Acetic Anhydride → HCID 9902340, compound

Participants

Reaction Steps

The compound of Step 1 (59 mg, 0.20 mmol) was dissolved in pyridine (1 ml) and acetic anhydride (2.0 mmol) was added. After stirring at room temperature for 20 hours the solvent was evaporated and the crude product was purified on silica (ethyl acetate:heptane 1:2). The title compound was obtained as a colorless oil (0.12 mmol).

Provenance & Evidence