HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 69592064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 69592095 | HCID 69592095 | — |
| Product | HCID 69592064 | HCID 69592064 | — |
Reaction Steps
Following the general method described in example 2b, 2-[2-(3-trifluoromethyl-phenyl)-vinyl]-pyridine 1-oxide was reacted first with dimethylsulfate and then with NaCN. After extraction and chromatography (SiO2 with CH2Cl2/MeOH=97/3) the title compound was obtained as a yellow oil and directly used in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07034044B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-252000636c3a47239a408b8af1d818bd |
| Source note | uspto-grants-2006_04 |