HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 22176442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 69592084 | HCID 69592084 | — |
| Product | HCID 22176442 | HCID 22176442 | — |
Reaction Steps
Following the general method described in example 2b, 2-methyl-4-styryl-pyridine 1-oxide was reacted first with dimethylsulfate and then with NaCN. After extraction and chromatography (SiO2 with CH2Cl2) the title compound was obtained as a yellow crystalline material. MS: m/e=220 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07034044B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-e68c1934d4f84d449381c7cc102c3907 |
| Source note | uspto-grants-2006_04 |