HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69617874, compound → HCID 69617814, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69617874 | HCID 69617874 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69617814 | HCID 69617814 | 85.4% |
Reaction Steps
A solution of 2-(3-nitrophenyl)furan-3-carboxylic acid methyl ester (1.0 g) in methanol (60 mL) containing 10% palladium on carbon (2.9 g) was stirred under 1 atmosphere of hydrogen for 1 h. The reaction mixture was then filtered through Celite. Removal of the solvent at reduced pressure gave the title compound as a yellow solid (0.75 g). C12H11NO3: M+Na+ 240
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07034053B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-76889fc5e3734590bad6d8399b7cdac6 |
| Source note | uspto-grants-2006_04 |