Triethylene Glycol → HCID 10267926, compound

HRID 1797283Notes

Reaction equation

HRID 1797283 reaction equation
[Br:1][C:2]1[CH:15]=[CH:14][CH:13]=[CH:12][C:3]=1[CH2:4][O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][OH:11].[CH2:16](O)[CH2:17][O:18]CCOCCO>>[Br:1][C:2]1[CH:15]=[CH:14][CH:13]=[CH:12][C:3]=1[CH2:4][O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][O:11][CH2:16][CH2:17][OH:18]

Participants

3

Reactant 2

HCID 8172Triethylene GlycolHCID 9965373HCID 9965373, compound

Product 1

HCID 10267926HCID 10267926, compound

Procedure

The compound was prepared and worked up as described in the preparation of compound 415, using triethylenglycol (16.0 mL, 120 mmol) instead of diethylenglycol. The crude product was purified by flash chromatography using DCM/acetone 6:1–3:1 as the eluent to afford the title compound as a pale yellow oil.

Workup

  1. customThe compound was prepared
  2. customThe crude product was purified by flash chromatography

Sources & evidence

ORD record
ord-35788ae04601472fa00716f5929c4912
Source dataset
uspto-grants-2006_04
Patent number
US07034015B2

Reaction notes

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