HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylene Glycol → HCID 10267926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylene Glycol | HCID 8172 | — |
| Reactant | HCID 9965373 | HCID 9965373 | — |
| Product | HCID 10267926 | HCID 10267926 | — |
Reaction Steps
The compound was prepared and worked up as described in the preparation of compound 415, using triethylenglycol (16.0 mL, 120 mmol) instead of diethylenglycol. The crude product was purified by flash chromatography using DCM/acetone 6:1–3:1 as the eluent to afford the title compound as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07034015B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-35788ae04601472fa00716f5929c4912 |
| Source note | uspto-grants-2006_04 |