6-Amino-1-hexanol → HCID 22174482, compound

Participants

Reaction Steps

The reaction and work up was conducted as described in the preparation of compound 205. Starting compounds were N-(5-bromo-2-{[3-chloro-4-(2-methylbenzoyl)phenyl]amino}phenyl)-succinamic acid (600 mg, 1.16 mmol) (prepared by a similar method as described in WO 01/05746) and 6-aminohexanol (151 mg, 1.28 mmol). The crude product was purified by flash chromatography using EtOAc as the eluent to afford the title compound as a yellow solid.

Provenance & Evidence