HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → Butyl prop-2-enoate;prop-2-enoic acid;styrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | Butyl Acrylate | HCID 8846 | — |
| Reactant | Sodium dodecylbenzene sulphonate | HCID 57371080 | — |
| Solvent | Water | HCID 962 | — |
| Product | Butyl prop-2-enoate;prop-2-enoic acid;styrene | HCID 168391 | — |
Reaction Steps
In a reactor equipped with a reflux condenser, a stirrer, a nitrogen-introducing pipe, and a monomer dripping funnel, 3.3 parts of sodium dodecylbenzenesulfonate is dissolved in 3,824 parts of ion exchange water. Subsequently, 30.6 parts of styrene, 9.4 parts of butyl acrylate, 1.2 parts of acrylic acid dimer, and 0.3 parts of dodecanethiol are added thereto, and thoroughly stirred at room temperature for emulsification stabilization (emulsified liquid 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343703B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-84a817739218448f800ce098b60147f5 |
| Source note | uspto-grants-2013_01 |