HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 178515184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl 4-Chloroquinoline-3-carboxylate | HCID 268963 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 178515184 | HCID 178515184 | — |
Reaction Steps
A suspension of ethyl 4-chloro-quinoline-3-carboxylate (3a) (2.35 g, 0.01 M) in 20 mL of o-xylene was refluxed with triethylamine (2.0 mL, 0.02 M) and phenyl hydrazine (2.89 g, 0.02 M) overnight. The crude product was obtained by filtration followed by washing the solid with cold methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343957B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-8ed176e5daa64842ae9a0ff5a8253e0e |
| Source note | uspto-grants-2013_01 |