Phenylhydrazine → HCID 178433617, compound

HRID 1797904Notes

Reaction equation

HRID 1797904 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]=[C:4]([CH3:12])[C:3]=1[C:13]([O:15]CC)=O.[C:18]1([NH:24][NH2:25])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[CH3:12][C:4]1[NH:5][C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:11]=2[C:2]2[C:3]=1[C:13](=[O:15])[N:24]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[N:25]=2

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 105386043-Quinolinecarboxylic acid, 4-chloro-2-methyl-, ethyl ester

Product 1

HCID 178433617HCID 178433617, compound

Procedure

The title compound was synthesized following the procedure described in step 3 using 3g and phenyl hydrazine. 1H NMR (DMSO-d6) δ (ppm): 2.77 (3H, s), 7.13 (1H, t, J=7.42 Hz), 7.45 (3H, m), 7.62 (2H, m), 8.20 (3H, m). m/z 276.4 (MH+).

Sources & evidence

ORD record
ord-c3bf410f4b324680b454c9db8da517fa
Source dataset
uspto-grants-2013_01
Patent number
US08343957B2

Reaction notes

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