HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 178515195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | Ethyl 4-chloro-6-(trifluoromethyl)quinoline-3-carboxylate | HCID 4322147 | — |
| Reactant | HCID 178515184 | HCID 178515184 | — |
| Product | HCID 178515195 | HCID 178515195 | — |
Reaction Steps
The title compound was prepared following the procedure described in Step 3 of the synthesis of 4a, using 3h and phenyl hydrazine. 1H NMR (DMSO-d6) δ (ppm):7.21 (1H, m), 7.42 (2H, t, J=7.56 Hz), 7.97 (1H, d, J=2.20 Hz), 8.00 (1H, d, J=2.20 Hz), 8.20 (1H, ddd, J=7.41, 1.10, 0.83 Hz), 8.43 (2H, dd, J=1.33, 0.83 Hz), 8.82 (1H, s). m/z 330.2 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343957B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-d664329faa5b4f7fa5abf36ff50b4b62 |
| Source note | uspto-grants-2013_01 |