HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(1,3-Dioxolan-2-ylmethyl)piperazine → HCID 57496168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(1,3-Dioxolan-2-ylmethyl)piperazine | HCID 2737195 | — |
| Reactant | 4-(3-(3-cyanophenyl)ureido)-N-(4-sulfamoylbenzyl)benzenesulfonamide | HCID 57496180 | — |
| Product | HCID 57496168 | HCID 57496168 | 43% |
Reaction Steps
The title compound was prepared from 4-(3-(3-cyanophenyl)ureido)-N-(4-sulfamoylbenzyl)benzenesulfonamide following procedure C and using 2.2 equivalent of 1-(1,3-dioxolan-2-ylmethyl)piperazine as secondary amine. The product was purified by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343963B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-93294267adda4a9d85414d99e58d4eba |
| Source note | uspto-grants-2013_01 |