HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 12568141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 13734994 | HCID 13734994 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12568141 | HCID 12568141 | 30% |
Reaction Steps
1-(hydroxymethyl)indole is prepared by reaction of 1-(pivaloyloxy-methyl)indole with sodium methylate in methanol at ambient temperature (yield: 30%) according to the procedure described in the following publication: D. Dhanak, C. B. Reese J. Chem. Soc., Perkin Trans. 1 1986, 2181-2186. It was characterized by mass spectrometry and by 1H and 13C NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343964B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-f2118abcfb964f05a5b53790572b95e3 |
| Source note | uspto-grants-2013_01 |