HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178484335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-Hydroxybenzamide | HCID 65052 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | HCID 178484335 | HCID 178484335 | — |
Reaction Steps
A solution of 4-hydroxybenzamide (5.58 g, 40 mmol) in 15 mL of dimethylformamide dimethyl acetal was stirred at 120° C. for 1.5 h with distillation of the product methanol. After cooling, the solid was collected and tritrarated with diethyl ether, DCM to give desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343990B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-66f5a7d0384b452ab560830aece1c90d |
| Source note | uspto-grants-2013_01 |