HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131730134, compound → HCID 131730135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131730134 | HCID 131730134 | — |
| Reactant | HCID 131730136 | HCID 131730136 | — |
| Product | HCID 131730135 | HCID 131730135 | — |
Reaction Steps
3-Chloro-6-(1-isopropylpiperidin-4-yl)pyridazine, hydrochloride (0.5 g, 1.6 mmol) and 2-methylpyridin boronic acid (0.241 g, 1.76 mmol) were mixed with catalyst and reacted in the same manner as in example 18. The title compound was isolated as white crystals of the trihydrochloride. Yield: 164 mg (25%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344001B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-85ee337a57f648d8bc775ea9940346f6 |
| Source note | uspto-grants-2013_01 |