HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanophenylboronic acid → HCID 59543425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanophenylboronic acid | HCID 2734326 | — |
| Reactant | HCID 59543436 | HCID 59543436 | — |
| Product | HCID 59543425 | HCID 59543425 | — |
Reaction Steps
1-(5-Bromopyridin-2-ylmethyl)-4-cyclobutylpiperazine (1.163, 3.75 mmol) and 4-cyanophenyl-boronic acid (0.82 g, 5.6 mmol) were mixed with catalyst and reacted in the same manner as in example 18. The title compound was isolated as white crystals of the free amine. Yield: 467 mg (44%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344001B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-8a73a05b50ba4cd9b5402b34733a9445 |
| Source note | uspto-grants-2013_01 |