HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanophenylboronic acid → HCID 25127136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanophenylboronic acid | HCID 2734326 | — |
| Reactant | HCID 59543436 | HCID 59543436 | — |
| Product | HCID 25127136 | HCID 25127136 | — |
Reaction Steps
1-(5-Bromopyridin-2-ylmethyl)-4-isopropylpiperazine (1.163, 3.75 mmol) and 4-cyanophenyl-boronic acid (0.82 g, 5.6 mmol) were mixed with catalyst and reacted in the same manner as in example 18. The title compound was isolated as white crystals of the free amine. Yield: 241 mg (20%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344001B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-351710f6b6e64a8492c46e511078c644 |
| Source note | uspto-grants-2013_01 |