Acetic Anhydride → N-(2-Phenyl-cyclopentyl)-acetamide

Beteiligte Stoffe

Reaktionsschritte

4.45 g of trans-2-phenyl-cyclopentylamine and 4.2 ml of triethylamine were dissolved in 50 ml of ethyl acetate. 2.86 ml of acetic anhydride was added slowly and the mixture stirred for 1 hour and washed with 40 ml of water. After drying the organic layer with sodium sulfate, filtration and evaporation 4.7 g of a crude solid was obtained that was used without further purification.

Herkunft & Nachweise