反应详情

4.45 g of trans-2-phenyl-cyclopentylamine and 4.2 ml of triethylamine were dissolved in 50 ml of ethyl acetate. 2.86 ml of acetic anhydride was added slowly and the mixture stirred for 1 hour and washed with 40 ml of water. After drying the organic layer with sodium sulfate, filtration and evaporation 4.7 g of a crude solid was obtained that was used without further purification.

1. washwashed with 40 ml of water
2. customAfter drying the organic layer
3. filtrationwith sodium sulfate, filtration
4. customevaporation 4.7 g of a crude solid
5. customwas obtained
6. customthat was used without further purification