HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → HCID 178492785, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | Clopyralid | HCID 15553 | — |
| Reactant | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| Reactant | HCID 178527894 | HCID 178527894 | — |
| Product | HCID 178492785 | HCID 178492785 | — |
Reaction Steps
Compound of Production Example 144 can be produced by the same method as Production Example 1, by a method according thereto, or by a combination of these and ordinary methods, with the use of 3,6-dichloro-2-pyridinecarboxylic acid, 2-amino-4,5-dimethyl-thiazole, 4-methoxy-thiophenol and 3-mercapto-1,2,4-triazole. 1HNMR (CDCl3) δ: 2.29 (3H, s), 2.33 (3H, s), 3.87 (3H, s), 6.98-7.03 (3H, m), 7.21 (1H, d, J=8.6 Hz), 7.48 (2H, d, J=8.6 Hz), 8.29 (1H, s) ESI-MS (m/e): 471 [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344003B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-a1862ccd7cee4451af99ab72b08777ac |
| Source note | uspto-grants-2013_01 |