HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylparaben → Benzoic acid, 4-[(2E)-2-buten-1-yloxy]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | trans-Crotyl alcohol | HCID 637922 | — |
| Product | Benzoic acid, 4-[(2E)-2-buten-1-yloxy]- | HCID 23321309 | 91.4% |
Reaction Steps
A reaction similar to that described in Example 1 (1a) was conducted using methyl 4-hydroxybenzoate (5.00 g, 32.9 mmol) and trans-crotyl alcohol (manufactured by Fluka, 2.37 g, 32.9 mmol) to give 5.78 g of the title compound (white powder, yield: 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344029B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-414aabce67944881819f211b8a8ecff2 |
| Source note | uspto-grants-2013_01 |