Hydrogen Sulfide → 1-(Pyridin-2-yl)ethane-1-thiol

HRID 1799521Notes

Reaction equation

HRID 1799521 reaction equation
[SH2:1].[S].[CH:3]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][N:6]=1)=[CH2:4]>>[N:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[CH:3]([SH:1])[CH3:4]

Participants

4

Reactant 3

HCID 402Hydrogen Sulfide2×HCID 75212-VinylpyridineHCID 5362487Sulfur

Product 1

HCID 202176771-(Pyridin-2-yl)ethane-1-thiol

Procedure

The reaction using hydrogen sulfide as the sulfur-containing compound is as follows. That is, vinyl pyridine is reacted with hydrogen sulfide to obtain pyridylethanethiol represented by the above general formula (3) as the pyridylethylthio compound.

Workup

  1. additioncontaining compound

Sources & evidence

ORD record
ord-012b39e4f27945619274bd6b2fb875d7
Source dataset
uspto-grants-2013_01
Patent number
US08344152B2

Reaction notes

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