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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1800438Generated: November 1, 2026

Potassium Carbonate → HCID 68419363, compound

https://huagongshe.com/reaction/1800438

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant2-Chloro-5-nitropyridineHCID 78308—
ReactantHCID 64793275HCID 64793275—
SolventDimethylformamideHCID 6228—
ProductHCID 68419363HCID 68419363—

Reaction Steps

In the same method as in Example C1(v), the title compound (8.35 g, 98%) was obtained as an orange oil using N-(3-hydroxy-4-methylphenyl)-3-(trifluoromethyl)benzamide (6.00 g, 20.3 mmol), 2-chloro-5-nitropyridine (3.22 g, 20.3 mmol), potassium carbonate (8.43 g, 60.9 mmol) and N,N-dimethylformamide (150 mL) as starting materials. The title compound was used for the next reaction without further purification operation.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08344135B2
Source datasetuspto-grants-2013_01
ORD IDord-f5973eafa9e14e5eb2586d05e23ddddb
Source noteuspto-grants-2013_01