HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 68419363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chloro-5-nitropyridine | HCID 78308 | — |
| Reactant | HCID 64793275 | HCID 64793275 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68419363 | HCID 68419363 | — |
Reaction Steps
In the same method as in Example C1(v), the title compound (8.35 g, 98%) was obtained as an orange oil using N-(3-hydroxy-4-methylphenyl)-3-(trifluoromethyl)benzamide (6.00 g, 20.3 mmol), 2-chloro-5-nitropyridine (3.22 g, 20.3 mmol), potassium carbonate (8.43 g, 60.9 mmol) and N,N-dimethylformamide (150 mL) as starting materials. The title compound was used for the next reaction without further purification operation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344135B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-f5973eafa9e14e5eb2586d05e23ddddb |
| Source note | uspto-grants-2013_01 |