HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-aminobenzoate → HCID 178498127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-aminobenzoate | HCID 12082 | — |
| Reactant | Benzyl 3-formylbenzoate | HCID 23286083 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178498127 | HCID 178498127 | — |
Reaction Steps
To a solution of methyl 4-aminobenzoate (7.94 g, 52.5 mmol) in ethanol (100 mL) was added benzyl 3-formylbenzoate in ethanol (50 mL) and the resulting mixture was stirred at room temperature for 2 h. The white solid precipitated was collected by filtration and washed with ethanol, dried in vacuo (50° C.) to give 15.6 g of (E)-benzyl 3-((4-(methoxycarbonyl)phenylimino)methyl)benzoate as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344137B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-926e191db5534e739a9d6227ecf3edde |
| Source note | uspto-grants-2013_01 |