Triethylamine → HCID 20199843, compound

HRID 1801401Notes

Reaction equation

HRID 1801401 reaction equation
[NH:1]([CH2:6][C:7]([OH:9])=[O:8])[CH2:2][C:3]([OH:5])=[O:4].[CH2:10]([N:12]([CH2:15][CH3:16])[CH2:13][CH3:14])[CH3:11]>CS(C)=O>[CH2:10]([N:12]([CH2:15][CH3:16])[CH2:13][CH3:14])[CH3:11].[NH:1]([CH2:6][C:7]([OH:9])=[O:8])[CH2:2][C:3]([OH:5])=[O:4]

Participants

4

Reactant 2

HCID 8471TriethylamineHCID 8897Iminodiacetic acid

Product 1

HCID 20199843HCID 20199843, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent2×

Procedure

3 g of iminodiacetic acid, 15 g of dimethyl sulfoxide, and 12 g of triethylamine were placed in a 500 mL capacity three-necked flask provided with a refluxing condenser, and stirred, thereby a dimethylsulfoxide solution of iminodiacetic acid triethylamine salt was obtained.

Workup

  1. customprovided with a refluxing condenser

Sources & evidence

ORD record
ord-bbfc3fea4a6743bd9c3b8157ffcb6456
Source dataset
uspto-grants-2013_01
Patent number
US08349031B2

Reaction notes

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