Ethanolamine → 1-Octyl-5-oxopyrrolidine-3-carboxylic acid

HRID 1801404Notes

Reaction equation

[CH2:1]([NH2:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:10]([OH:18])(=[O:17])[C:11]([CH2:13][C:14](O)=[O:15])=[CH2:12].C(CN)O>>[CH2:1]([N:9]1[C:14](=[O:15])[CH2:13][CH:11]([C:10]([OH:18])=[O:17])[CH2:12]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

Reactant 3

HCID 700Ethanolamine

HCID 811Itaconic acid

HCID 8143Octylamine

Product 1

HCID 940891-Octyl-5-oxopyrrolidine-3-carboxylic acidYield 125.8%

Procedure

129 g of octylamine, 130 g of itaconic acid and 61 g of monoethanolamine were used to obtain 303 g of N-octyl-5-oxopyrrolidine-3-carboxylic acid monoethanolammonium salt with

Sources & evidence

ORD record: ord-4cf5022447c4478ea1f45bab6a5bebcd
Source dataset: uspto-grants-2013_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08349215B2

Reaction notes

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