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HRID1801453

反应详情

EQUATION

反应方程式

HRID 1801453 的结构方程式

REACTANTS

反应物

2
结构：CCOc1ccc(N)cc1
HCID9076

4-Ethoxyaniline

C8H11NO

结构：CC(C)(C)[Si](C)(C)OCC[C@@H]1CO1
HCID11217932

未命名化合物

PRODUCTS

生成物

1
结构：CCOc1ccc(NC[C@H](O)CCO[Si](C)(C)C(C)(C)C)cc1
HCID67131106

未命名化合物

收率 62%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Starting from 4-ethoxyaniline (3.2 mL; commercial) and tert-butyl-dimethyl-((R)-2-oxiranyl-ethoxy)-silane (5.0 g; prepared according to WO 2007/144423) and following procedure A, the title compound was obtained after CC (EA/Hept 1:1) as a brown oil (5.22 g; 62% yield).