Ethyl Acrylate → HCID 68629375, compound

HRID 1801454Notes

Reaction equation

HRID 1801454 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][C:9](=[O:13])[NH:10]2)=[CH:5][CH:4]=1.[C:14]([O:18][CH2:19][CH3:20])(=[O:17])[CH:15]=[CH2:16]>>[CH2:19]([O:18][C:14](=[O:17])[CH2:15][CH2:16][N:10]1[C:11]2[C:6](=[CH:5][CH:4]=[C:3]([O:2][CH3:1])[CH:12]=2)[CH:7]=[CH:8][C:9]1=[O:13])[CH3:20]

Participants

3

Reactant 2

HCID 8821Ethyl AcrylateHCID 299427567-Methoxy-1,2-dihydroquinolin-2-one

Product 1

HCID 68629375HCID 68629375, compoundYield 100%

Procedure

The compound was obtained according to procedure H starting from 7-methoxy-2(1H)-quinolinone (614 mg, 3.5 mmol) and ethyl acrylate (0.4 mL). The crude brown oil (0.96 g; 100% yield) was used as such in the next step.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-3abc3dfe55d4468a8bb9b1059b849c05
Source dataset
uspto-grants-2013_01
Patent number
US08349826B2

Reaction notes

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