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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1802301Generated: October 27, 2026

tert-Butyl carbamate → HCID 67774056, compound

https://huagongshe.com/reaction/1802301

Reaction equation

Participants

RoleNameHCIDCharge
Reactanttert-Butyl carbamateHCID 77922—
Reactant7-Bromo-2-(6-fluoropyridin-2-YL)-[1,2,4]triazolo[1,5-A]pyridineHCID 67774331—
ProductHCID 67774056HCID 6777405632.5%

Reaction Steps

The product was prepared in the same manner as described in example 1c using 7-bromo-2-(6-fluoropyridin-2-yl)-[1,2,4]triazolo[1,5-a]pyridine (1.44 g, 4.91 mmol) and tert-butyl carbamate (691 mg, 5.9 mmol) as starting materials. The reaction affords [2-(6-fluoro-pyridin-2-yl)-[1,2,4]triazolo[1,5-a]pyridin-7-yl]-carbamic acid tert-butyl ester (526 mg, 32.5%), as off-white crystals. MS: m/z=330.0 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08349824B2
Source datasetuspto-grants-2013_01
ORD IDord-667468a434a24f5ea761bfc4b1e02594
Source noteuspto-grants-2013_01