HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbamate → HCID 67774056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbamate | HCID 77922 | — |
| Reactant | 7-Bromo-2-(6-fluoropyridin-2-YL)-[1,2,4]triazolo[1,5-A]pyridine | HCID 67774331 | — |
| Product | HCID 67774056 | HCID 67774056 | 32.5% |
Reaction Steps
The product was prepared in the same manner as described in example 1c using 7-bromo-2-(6-fluoropyridin-2-yl)-[1,2,4]triazolo[1,5-a]pyridine (1.44 g, 4.91 mmol) and tert-butyl carbamate (691 mg, 5.9 mmol) as starting materials. The reaction affords [2-(6-fluoro-pyridin-2-yl)-[1,2,4]triazolo[1,5-a]pyridin-7-yl]-carbamic acid tert-butyl ester (526 mg, 32.5%), as off-white crystals. MS: m/z=330.0 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08349824B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-667468a434a24f5ea761bfc4b1e02594 |
| Source note | uspto-grants-2013_01 |