HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbamate → HCID 67777207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbamate | HCID 77922 | — |
| Reactant | HCID 67774606 | HCID 67774606 | — |
| Product | HCID 67777207 | HCID 67777207 | 55.2% |
Reaction Steps
The product was prepared in the same manner as described in example 8e using 7-bromo-N-cyclopropyl-N-methyl-[1,2,4]triazolo[1,5-a]pyridin-2-amine (540 mg, 2.02 mmol) and tert-butyl carbamate (284 mg, 2.43 mmol) as starting materials. The reaction affords [2-(cyclopropyl-methyl-amino)-[1,2,4]triazolo[1,5-a]pyridin-7-yl]-carbamic acid tert-butyl ester (338 mg, 55.03%) as light yellow crystals. mp: 323.1° C., MS: m/z=397.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08349824B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-a8f14bcaa38045708fded4d60175c81a |
| Source note | uspto-grants-2013_01 |