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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1802306Generated: October 30, 2026

tert-Butyl carbamate → HCID 67777207, compound

https://huagongshe.com/reaction/1802306

Reaction equation

Participants

RoleNameHCIDCharge
Reactanttert-Butyl carbamateHCID 77922—
ReactantHCID 67774606HCID 67774606—
ProductHCID 67777207HCID 6777720755.2%

Reaction Steps

The product was prepared in the same manner as described in example 8e using 7-bromo-N-cyclopropyl-N-methyl-[1,2,4]triazolo[1,5-a]pyridin-2-amine (540 mg, 2.02 mmol) and tert-butyl carbamate (284 mg, 2.43 mmol) as starting materials. The reaction affords [2-(cyclopropyl-methyl-amino)-[1,2,4]triazolo[1,5-a]pyridin-7-yl]-carbamic acid tert-butyl ester (338 mg, 55.03%) as light yellow crystals. mp: 323.1° C., MS: m/z=397.1 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08349824B2
Source datasetuspto-grants-2013_01
ORD IDord-a8f14bcaa38045708fded4d60175c81a
Source noteuspto-grants-2013_01