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HRID1802997

反应详情

EQUATION

反应方程式

HRID 1802997 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCN
HCID8102

Hexylamine

C6H15N

结构：CC(C)(CCC(C)(C)OC(=O)CCl)OC(=O)CCl
HCID58282150

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCNCC(=O)OC(C)(C)CCC(C)(C)OC(=O)CNCCCCCC
HCID86653836

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The cleavable diol is made by the following manner. Compound (61) is reacted with 5 equivalents of 1-aminohexane (65) in methylene chloride. Wash with brine and dry to yield 2,5-dimethylhexane-2,5-diyl bis(2-(hexylamino)acetate) (66).

WORKUP

后处理

  1. washWash with brine
  2. customdry